Why can we use our BDG to make soap? If you are like the rest of us that make biodiesel, your biodiesel glycerin (BDG) may be piling up adding to the proverbial glycerin lake. This video discusses how to find your soap content in a biodiesel sample by using a soap titration. Plus, the moisturizing attributes of glycerin found in this soap are great for the skin. Measure the proper amounts of water and lye to be used, heat the water to 100 degrees F., add the lye and mix until all the lye is dissolved. If you have ever made bar soap from BDG you may have found that it can be fairly soft unless the oil you used to make your biodiesel came from saturated oils such as coconut, lard, tallow or hydrogenated vegetable oil. Reply Other Steps in Making Biodiesel Making good biodiesel requires several other steps besides the transesterification reaction. Stick with less than 15 percent in your overall recipe to avoid an overly soft soap bar. The process for making biodiesel uses an oil, a catalyst, and an alcohol. Not what we're shooting for here. But the ethanol has to be anhydrous -- free of water -- which can't be achieved by distillation. In this article will dig into the nitty gritty of what it takes to get started turning your nasty black stuff into bars or jars of this incredible soap! Heat the glycerin in a stainless steel or aluminum pot (or your bio processor) to 150 degrees F. to remove any excess methanol (if you used ethanol, heat to 175 F.). I filter mine down to 50 microns. The main byproduct of biodiesel is glycerin. http://www.knicenclean.com/recipes/recipes.html, HI In a small jar, dissolve. Everyone Ive ever spoken with reports that once they give a few bars out, the folks that they gave it to come back & want more and more of it. Change after adding methanol: murky fat (normal -- this is procedure). Secondly, it will ensure that all of the ingredients in the BDG are reacted into soap, otherwise you can end up with a soap that feels oily and cleans poorly. For 1 gallons of glycerin, use a 28-qt. Plus, itll help you get rid of that nasty barrel (or barrels) of glycerin you have laying around and hey, it may even earn you bonus points with those around you that tolerate your Biodiesel production hobby. I personally have been using Biodiesel glycerin soap in the shower for well over a year now and absolutely love it! Divide the weight by 100 to get the density. Methanol is at about $5 a gallon. So, what are you waiting for? This is a .01N solution. 9) Allow them to cure (2-3 weeks) If youve never tried using soap made from Biodiesel glycerin, youre really missing out. Youll be amazed how well it works! In addition to saponifiable elements, BDG already contains soaps that were created during the biodiesel production process. Also due to vegetable oil being renewable, the . hi sirmy name is ashok kumar mohapatra.i read your article.it is very helpful for me to make my biodiesel projectif u will help me regarding this within low budgetthen i can start my projectthank u. Makes you wonder what would it take to get people to ride bikes instead. You need to learn to make these 5 items After a careful study I could detect that these five items could be significant to be stockpiled, or even better, homemade: Vegetable oil Vinegar Biodiesel Soap and toothpaste Alcohol Lets see why I have identified these as important. This recipe can be hot processed (HP) or cold processed (CP). Biodiesel is a mixture of alkyl esters and it can be used in conventional compression ignitions engines, which need almost no modification. Nows a great time to start getting rid of that glycerin lake sitting out back & turning it into not only something worthwhile to clean with but possibly even a marketable product! I have on clean carboy I put some oil in, and put the rest in another bucket. 5) Pour the mixture into the molds and smooth it out Go have lunch. Required fields are marked *. (1 gallon of methanol per 5 gallons of oil and so on. As well, biodiesel can be used as heating oil and as fuel (Mushrush et al., 2001; Wardle, 2003). Place the glycerin in a stainless steel pot and heat it to 150 F (66 C) to remove any traces of methanol. BE CAREFULI use a chemical resistant p100 respirator when I do this process, as well as eye protection. It has water in it, and will ruin your reaction, avoid using this at all costs. 16 oz. Palm Oil 32 oz. Simple Steps to Making Biodiesel 1. On the other hand, soap formation Hook this up the same way you did the carboy with the oil. =). Using the black crown soap guide we have been able to make a terrific quality bar and liquid soap that both lather quite well. It needs to be Re-Batched. Let it sit with the element on for the next 12-14 hours. Next, you mix about 1100 grams of sodium hydroxide into the methanol. At this point you've drained the glycerin and have reached the fuel. I get a lot of questions about soap and toiletries. Heat the oil to 130 degrees F. (you can open the drain valve, get a quick sample, and use a quick-read thermometer to check. ) You will get arrested and get in a pile of trouble if you just take the oil. Strain the glycerin to remove any impurities and then return it to the pot. . Please don't run unwashed fuel in your car, and please don't forget to dry/filter after you wash. Now I know some of you are wondering about this, and yes, I am going to add a methanol recovery system. If youd like to learn more about this guide, click here. If youd like to just try a bar of this great soap to see what all the fuss is all about,we have a full line of various bars in different scents that you can purchase right from our website and give it a try. Your SAP may very -- Please obtain a SAP specific to your glycerin and always check the final pH of your soap. To get the most accurate results, it's best to check the density of your biodiesel. Cover the liquid with a piece of plywood or cardboard to help hold the heat in so the soap cures properly. Biodiesel will run in a diesel engine, I don't recommend trying it in a gas engine. Image titled Make Lye Soap from Biodiesel By products Step 9 Cut the soap into 45 bars that measure 3-by-2 inches (5.1 cm). Liquid Glycerin Lye 9.4 oz. Most fast food places burn their oil. Theres a really good example here: 10 years ago 2022 Soap Queen Site Design by Emily White Designs, The best soap supplies on the internet are found at Bramble Berry. Some may say that lather is just eye candy for cleaning but that is not totally true. About: Ask me questions. End of acid stage (note darker colour). Give it a try! ). Use this recipe to customize your own handmade flower soap using lavender, rose-geranium, ylang ylang, or another flower essential oil. The first step would be to accurately weigh the lard and lye using the scale, and the water using. My wife wont ever TOUCH that stuff! This article is written by Rick Knicely from the Knice-N-Clean Soap Company. There are several people (including us) that sell Biodiesel glycerin soap on a regular basis. Also, be sure to have the vent on the back of the carboy open, or you'll create a vacuum and the carboy will implode. First and foremost, it keeps you from making caustic hot soap which can range from a minor irritant to just plain dangerous. By adding other whole oils or fatty acids you can add the missing properties to your BDG soaps to create the desired soap you want to create. If you're using more than 5 gallons of oil you obviously will need to disconnect the hose and repeat more than once. If using pre-dilution method subtract the pre-dilution water from the final dilution water. This is where balancing your soap comes in. Vegetable Oil NOW Close the intake valve.Double check the pressure vent on the processor. The water content of acid oils was 3.15% and 0.8%. Once it turns bright pink and stays that way you need to count exactly how many milliliters of lye/water solution you used to neutralize the acidity of the oil. I do not personally recommend making soap with the byproduct glycerin from biodiesel manufacturing as I dont think its entirely clean and pure and has some extra things like methanol in it. 10. Everything from green liquid hand soap to sparkly colored bars to tips & tricks on how to get your soap to do just about anything under the sun are discussed on a regular basis. on Introduction. The Mixture will separate into a light top layer of bio diesel and a darker bottom layer of glycerin, soap and catalyst. my basic setup is very low tech, just a bag filter hung from a broom stick over a clean bucket. Take a carboy filled with oil and connect a section of hose from the carboy to the intake valve on your processor. 11. NaOH is cheaper, and that's why I went with it.-Methanol Methanol is used for race car fuel, and can be purchases at many chemical supply places. FYIIn the photo the biodiesel is on the right and the glycerin is on the left. Biofuels from food crops- bad idea, biofuels from non-food sources- the way of the future. No harvesting required. So if you think about it, in a way, our BDG is already soap. This is actually incorrect. F. Keep stirring until the bubbles quit coming up. 1) Fill a clean glass jar half-way full of Biodiesel 2) Fill the rest of the jar with distilled water 3) Cap the jar and shake it vigorously for about 10 seconds 4) Set the jar down and allow the water and Biodiesel to sit for about 30 min to 1 hour 5) Return and look at the water that has settled to the bottom. Please read up on this before you start, and please understand the chemical dangers involved in this process. Purer methanol means better biodiesel and less soap in the biodiesel process. Biodiesel is a great way to go green, and cut your carbon footprint quite substantially, not to mention it's cheaper than diesel. Anybody experienced with this? Biodiesel From Used Kitchen Grease or Waste Vegetable Oil by Mike Pelly This is how to make your own biodiesel fuel from used cooking oil. Finally pour off the biodiesel from the top of the container. Unless stated otherwise, all images are original material and are copyrighted. 7. Open the valve nearest the tank and make sure the valve on the other side of the drain is closed, then slowly open the drain valve. The design takes waste methanol/water vapor that is released during the reaction within the UR Biodiesel process and purifies it to over 95% methanol. So, What gives? Glycerin is a natural byproduct from the biodiesel refining process. Pingback: Making Soap From Biodiesel Glycerin | Utah Biodiesel Supply Blog | Soap, Soap making is a great option for anyone wanting to do more for themselves. bucket. Add this mixture to the oil and stir vigorously. 3) Add the catalyst/water solution to the heated glycerin while stirring 4. It can do some serious bodily damage. Technical information: 1lb / 454g batch 5% superfat 33% water discount. 2) Dissolve some catalyst (NaOH or KOH) and water in a bowl ). The project will also make the biodiesel lab more sustainable so the students can reuse methanol rather than purchase . on Introduction, Reply personally I have seen plenty of swimming pools and ponds that could use to have some cleaning done at least there the algae could be used rather than just thrown / flushed away if algae harvesting was easy to do. I will do my next instructable on dry-washing biodiesel. Continued mixing 30 - 60 minutes until the yield remains constant. Another tool you can use is the KNC Soap Calculator which will help you formulate a balanced recipe for your BDG that will give you a nice firm bar soap and/or bar and liquid soap with tons of lather. It can also be used in the sink to clean the dishes too. Pour the oil into a. For the actual making of the fuel you will need:- an appleseed processor-WVO (you'll get as much fuel as the amount of WVO you use) You can get this from restaurants, but you need their OK before you take it. 3. Click. Step two: Build your plant, sized to your feedstock supply. Avocado oil: A nourishing and moisturizing oil that lends a slightly green (or yellowish) hue to soap. 11 years ago Now open the valve on the carboy and the intake valve. One word: Algae. The size and number of containers needed depends on the amount of glycerin you are using and the desired thickness of the soap. Whether you sell it to your friends & neighbors, market it at fairs & bazaars or sell it on the web, once people get a hold of some, they always seem to come back for more. Did you make this project? For NaOH, the commonly accepted amount is 5 grams of NaOH per 1 liter of vegetable oil to be converted. Probably not a bad idea, and I may do this in the future. Dump the catalyst into the carboy and immediately screw on the same lid or same kind of lid as shown in the previous step, the one with a ball valve on it. Image titled Make Lye Soap from Biodiesel By products Step 3 Stearic acid, palmetic acid, myristic acid and lauric acid are all available in flakes and can be used in addition to or in place of the saturated oils to better tailor your recipe. Weigh out 100 ml of biodiesel on your pocket scale. The recipe above will be soft but will lather decently and last much longer than 100% glycerin soap. 5. Check out pictures of peoples soap here. I was looking to make more of a shop soap/cleaner soap with this but I know there is a bit of controversy over it. It may still be caustic and you should perform a ph test. place plastic container in ice bath. Palm Oil The soaps ph level should be less then 10. Add the water and lye mixture to the glycerin. I used an old sock to get out the large particles before it went through the filter. QUICK DIY BIODIESEL GLYCERIN BAR SOAP - 12 MINUTE HOT PROCESS GLYCERIN SOAP HANDMADE & HOMEMADE - During the process of making biodiesel biofuel you are lef. Finally the SAP value will take the guess work out of the process and allow you to make consistent soaps, batch after batch. If you can make Biodiesel, making soap will be a breeze! Tilt the carboy to make sure all the methoxide drains out. But you know I use biofuel for most of my transport needs: I eat food and ride a bike. The formula is this: For NaOH- # of liters of oil x 4 grams + titrationFor example, say I titrated at 2 milliliters and was using 50 liters of oil. (now, I've tried to make this neutral enough so that I don't spark a huge debate, but, in advance, sorry if i offend anyone). A SAP value is important for a number of reasons. Available on the market today are several soap making fragrances that can be added to give the soap practically any scent youd like. Ive personally seen it take out some of the worst stains out of kids clothes that commercially bought soap detergents couldnt even touch. Warm a liter of your. It will cause blindness or death if ingested; one way it's absorbed into your body is through your skin, so simply handling the stuff with bare hand is bad for you. The hydroxide ion implies the presence of water in the system. Instructable #2 in my series on biodiesel. This still ends up being cheaper than regular diesel, since you add 20% methanol for the amount of WVO you use.Safety equipment you'll need:-chemical resistant p100 respirators Got 2 at Lowes for $25-$30 each-lab goggles-chemical resistant glovesWhat you'll need for the titration:-Isopropyl alcohol get this at an auto parts store-distilled water-a very tiny bit of your catalyst (NaOH or KOH)-a sample of your WVO-3 oral syringes Get these at the drug store-Phenol Red indicator (like for testing your pool water). You can do one of two things: 1. Heat it to 175 F (79 C) if you made your biodiesel from ethanol. Youll be squeaky clean sooner than you think! 6) Shake the molds back and forth to allow it to settle. Prepare your biodiesel in a well-ventilated area. we have a full line of various bars in different scents that you can purchase right from our website and give it a try. Make sure it's all very tight and secure, you don't want this stuff leaking. example 1, The other way is to put it under vacuum and use a methanol recovery still to get it all out. Leave the element on. Were pretty sure that once you try it youll want more and will be just as hooked on the stuff as we are. container to make 1 -inch-thick soap. Converting Used Oil and Trap Grease to Biodiesel When a feedstock contains less than 3% or 4% FFA, most people just add extra catalyst, let the FFAs convert to soap, and then remove the soap. 7 years ago I am posting my thoughts on this interesting subject for all to see, in the hopes that it educates and possibly stems the endless tide of I know this is a really strange question, but I make biodiesel and I was wondering . emails. 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